GEt Quote

Thermal Test of Coatings

As low as $550.00 $0.00
In stock
SKU# ASTT03

~mm to sub-um thick

Product Detail

ACS Material's photothermal testing service measures the thermal conductivity and interface thermal resistance of coatings on their own substrate. A modulated laser heats the surface and an infrared detector reads its thermal radiation. The service needs one specimen, millimeter to sub-micrometer thick and more than 3 mm across, and runs at room temperature. Typical lead time is 1 week.

Check your sampleCompare your specimen with this service and get an inquiry ready to send.
Measures
Thermal conductivity, interface thermal resistance
Method
Photothermal, modulated laser
Thickness
~mm to sub-µm
Size
More than 3 mm across
Specimens
1, non-returnable
Temperature
Room temperature
A modulated laser heats a coating, topped with a thin gold film, on its substrate; an infrared detector reads the thermal radiationA modulated laser heats the surfaceModulated laserIR detectorCoatingSubstrateGold filmHeat reaches deeper at lower frequencyPhase shift of the surface temperature versus modulation frequency, from a heat-conduction modelWhat the detector records0°−15°−30°−45°Modulation frequency (log scale)Phase shiftLow frequency:heat reachesthe substrateHigh frequency:heat stays in the coatingμ = √(α / (πf)): thermal penetration depth
A laser switched on and off at a set frequency heats the gold-coated surface, and the detector reads how far the surface temperature lags behind. The curve is an illustrative model response for a low-conductivity coating on a high-conductivity substrate, not measured service data; its shape depends on the specimen and the model.

How the measurement works

We first coat the surface with a thin gold film. A laser beam, switched on and off at a set frequency, then heats the surface. The surface temperature follows the heating with a delay, and an infrared detector reads it through the thermal radiation of the surface. The delay, read as a phase shift, is measured over a range of modulation frequencies. At high frequencies the heat stays near the surface, inside the coating; at lower frequencies it reaches the interface and the substrate. Fitting a heat-conduction model to the phase curve gives the coating's thermal conductivity through its thickness and the interface thermal resistance. The thin-film guide explains why a film's conductivity along its plane can differ.

Is this the right service?

Your sampleService
Free-standing wire, fiber or film, micrometer thickMicrometer-thick service
Free-standing wire, fiber or film, thinner than a micrometerSub-micrometer service
A coating on its substrate, sub-micrometer to millimeter thickThis service
A 2D layer, tens of nanometers or thinner2D materials service
A bulk piece, tens of micrometers to tens of centimeters thickBulk materials service

Specimens outside these limits are worth describing before you ship them. All five services are compared on the thermal testing services page.

Check your sample

Enter your specimen and what you need. The checker compares it with the numbers listed for each service, marks what it cannot compare, and writes an inquiry you can send as it is.

Sending specimens

One specimen, more than 3 mm acrossThe coating stays on its substrate. Specimens are non-returnable.
Coating thicknessGive the thickness and how it was measured; the model needs it.
SubstrateName the substrate material and its thickness.
Coated side markedProtect the coated surface in transit and mark which side is coated. We apply the thin gold film for the measurement ourselves; tell us about any existing surface layers or treatments.

FAQ

Can you measure the coating without its substrate?

This service measures the coating on its substrate, through its thickness. A free-standing film fits the TET services, which measure along the film: the micrometer-thick service, or the sub-micrometer service for thinner films.

Does the coating need to conduct electricity?

No. The laser heats the surface and the detector reads its thermal radiation, so nothing is wired to the specimen. Conducting and insulating coatings are measured the same way.

Which temperature is the test run at?

Room temperature. If you need another temperature, describe it with the sample checker before ordering.

How do I order?

Choose Room Temperature in the Type menu at the top of this page and add the test to the cart. Then check out, or click GET A QUOTE in the cart to request a quote. For a specimen outside the listed requirements, send the details first with the sample checker.

How thin can the coating be?

The listed range is millimeter to sub-micrometer thick, on a specimen more than 3 mm across. For a coating near the thin end, send its thickness and substrate first with the sample checker.

Related guides

Thin-Film Thermal Conductivity: In-Plane vs. Cross-Plane — why one number is never enough for a film.
Interfacial Thermal Resistance: The Invisible Wall Inside Every Stack — where the resistance comes from and how it is measured.
Time-Domain Thermoreflectance (TDTR) Explained — the optical method for nanometer films and buried interfaces.
Which Thermal Measurement Method Should You Use? — choose by sample form, support state and scale.
Thermal Testing Sample Preparation Guide — geometry, mounting and conditioning.

Disclaimer: ACS Material LLC believes that the information on our website is accurate and represents the best and most current information available to us. ACS Material makes no representations or warranties either express or implied, regarding the suitability of the material for any purpose or the accuracy of the information listed here. Accordingly, ACS Material will not be responsible for damages resulting from use of or reliance upon this information.