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Thermal Test of Bulk Materials

As low as $550.00 $0.00
In stock
SKU# ASTT04

tens of μm to tens of cm thick

Product Detail

ACS Material's photothermal testing service measures the thermal conductivity of bulk materials, from tens of micrometers to tens of centimeters thick. A modulated laser heats the surface and an infrared detector reads its thermal radiation. The service needs one specimen, more than 2 mm across, and runs at room temperature. Typical lead time is 1 week.

Check your sampleCompare your specimen with this service and get an inquiry ready to send.
Measures
Thermal conductivity
Method
Photothermal, modulated laser
Thickness
Tens of µm to tens of cm
Size
More than 2 mm across
Specimens
1, non-returnable
Temperature
Room temperature
A modulated laser heats a gold-coated bulk specimen; an infrared detector reads the thermal radiationA modulated laser heats the surfaceModulated laserIR detectorBulkspecimenGold filmHeat reaches deeper at lower frequencyPhase shift of the surface temperature versus modulation frequency, from a heat-conduction modelWhat the detector records0°−15°−30°−45°Modulation frequency (log scale)Phase shiftLow frequency:heat spreadswide and deepHigh frequency:heat stays near the surfaceμ = √(α / (πf)): thermal penetration depth
A laser switched on and off at a set frequency heats a small spot on the gold-coated surface, and the detector reads how far the surface temperature lags behind. The curve is an illustrative model response for a laser spot on a thick specimen, not measured service data; its shape depends on the specimen and the model.

How the measurement works

We first coat the surface with a thin gold film. A laser beam, switched on and off at a set frequency, then heats a small spot on it. The surface temperature follows the heating with a delay, and an infrared detector reads it through the thermal radiation of the surface. The delay, read as a phase shift, is measured over a range of modulation frequencies. At low frequencies heat spreads wide and deep before each cycle ends; at high frequencies it stays near the surface. Fitting a heat-conduction model to the phase curve gives the thermal conductivity. Heating and reading happen on the same face. The laser flash guide covers the usual bulk method and its limits.

Is this the right service?

Your sampleService
Free-standing wire, fiber or film, micrometer thickMicrometer-thick service
Free-standing wire, fiber or film, thinner than a micrometerSub-micrometer service
A coating on its substrate, sub-micrometer to millimeter thickCoatings service
A 2D layer, tens of nanometers or thinner2D materials service
A bulk piece, tens of micrometers to tens of centimeters thickThis service

Specimens outside these limits are worth describing before you ship them. All five services are compared on the thermal testing services page.

Check your sample

Enter your specimen and what you need. The checker compares it with the numbers listed for each service, marks what it cannot compare, and writes an inquiry you can send as it is.

Sending specimens

One specimen, more than 2 mm acrossTens of micrometers to tens of centimeters thick. Specimens are non-returnable.
Size and thicknessGive the dimensions of the piece, including its thickness.
Composition and processingGive the material, its composition, and how the piece was made or treated.
Surface as receivedWe apply the thin gold film for the measurement ourselves; tell us about any existing surface layers or treatments. Protect the faces in transit and label the specimen.

FAQ

What size and thickness can the specimen be?

The listed range is tens of micrometers to tens of centimeters thick and more than 2 mm across, one specimen. A thin layer on a substrate fits the coatings service.

Which temperature is the test run at?

Room temperature. If you need another temperature, describe it with the sample checker before ordering.

Does the material need to conduct electricity?

No. The laser heats the surface and the detector reads its thermal radiation, so nothing is wired to the specimen.

How do I order?

Choose Room Temperature in the Type menu at the top of this page and add the test to the cart. Then check out, or click GET A QUOTE in the cart to request a quote. For a specimen outside the listed requirements, send the details first with the sample checker.

How is this different from laser flash?

Laser flash heats one face of a thin disc with a single pulse and reads the temperature on the opposite face, and the disc usually has to be machined to the instrument's size. Here the heating and the reading are both on the same face. The laser flash guide covers the flash method and its limits.

Related guides

Laser Flash Analysis (LFA) Explained — the standard bulk method, and where it fails.
Transient Plane Source (Hot Disk / TPS) Explained — the sensor-between-two-pieces method.
Thermal Conductivity vs. Thermal Diffusivity — the difference that decides your measurement.
Steady-State vs. Transient Thermal Measurement — two philosophies, one property.
How to Read a Thermal Test Report — what a defensible report states.

Disclaimer: ACS Material LLC believes that the information on our website is accurate and represents the best and most current information available to us. ACS Material makes no representations or warranties either express or implied, regarding the suitability of the material for any purpose or the accuracy of the information listed here. Accordingly, ACS Material will not be responsible for damages resulting from use of or reliance upon this information.