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  • Heat Sealing and Vacuum-Assisted Joining: Process Variables for Thin-Film Samples

    Oct 24, 2026 | ACS MATERIAL LLC

    Heat sealing and vacuum-assisted joining are used in thin-film labs to close pouches, bond cover sheets and press stacks together. The joint depends on the temperature reached at the interface, a modest contact pressure, enough dwell time and a clean, compatible interface. This guide explains those variables, what vacuum can and cannot do, how sealing differs from laminating, and how to qualify a joint.

    Heat sealing: the formation of a joint between two layers by bringing them together between heated platens, so that a thermoplastic interface melts, wets and solidifies [1].

    In one paragraph: For polyethylene films, seal properties were set mainly by the maximum interface temperature; dwell only had to be long enough to reach it, and slight pressure for contact was enough [2]. Seal initiation tracks the melting behaviour of the polymer [1]. Vacuum reduces trapped gas but does not guarantee a void-free joint [4]. Seal strength (ASTM F88) is not barrier performance [3][5].

    Coated glass sample vacuum-laminated between two clear polymer films with a heat-sealed margin
    A sample sealed between two films. Illustration, not a specific instrument.

    1.  What Heat Sealing and Vacuum-Assisted Joining Are

    Heat sealing joins two layers by bringing them into contact under heat and pressure for a set time, so that a thermoplastic layer at the interface softens or melts, wets the opposite surface and solidifies into a joint. Stehling and Meka describe it, for polymer films, as the formation of a joint between two films by placing them briefly between heated platens [1]. Vacuum-assisted joining adds one more element: the air between the layers is pumped out before or during pressing.

    In a thin-film laboratory the same physics appears in several jobs: closing a pouch or bag around a sample, bonding a cover film or sheet to a coated substrate, or pressing a stack of layers together. This guide covers the process variables that control the joint, what vacuum does and does not do, how sealing differs from laminating, and how to check that a joint is reproducible. It is not a validated recipe for any particular material stack.

    2.  Temperature, Pressure, Dwell Time and the Interface

    Four variables control a heat-sealed joint: temperature, pressure, dwell time and the interface itself. Meka and Stehling measured the interfacial temperature during sealing of polyethylene films with micro-thermocouples, compared it with finite element calculations, and quantified how seal bar temperature, dwell time and pressure affected seal strength, elongation and seal energy [2]. Their findings for those films are a useful frame:

    VariableWhat the study found for polyethylene films [2]Practical reading
    TemperatureSeal properties are determined primarily by the maximum temperature reached at the interfacePlaten set-point is not interface temperature; heat must pass through the outer layers first
    Dwell timeMust be long enough to bring the interface to the desired temperature; longer times at a given interfacial temperature did not improve seal propertiesThicker or less conductive stacks need longer dwell to reach the same interface temperature
    PressureA slight pressure helped bring the surfaces into contact; higher pressure did not improve seal properties in the studyFor these polyethylene films, higher pressure did not improve seal properties; qualify pressure for other materials
    Excess heatIncreased pressure and dwell at temperatures above the final melting point were detrimental to seal appearance due to deformationExcess heat, pressure and dwell can deform the joint; qualify the process for the material

    Summary of Meka and Stehling [2]; results apply to the polyethylene films and conditions studied.

    The second paper in the same series linked sealing temperature to the melting behaviour of the polymer. For polyethylene films, the seal initiation temperature corresponded to the temperature at which the amorphous fraction reached 77±3%; seal strength then rose with the amorphous fraction and reached a plateau at the final melting point, with the plateau strength set by the yield stress of the film [1]. The practical message is that a sealing window should be found from the material’s melting behaviour and a temperature series, not assumed from another material.

    The interface

    Contamination, moisture, surface texture and the compatibility of the two surfaces all affect whether molten polymer wets and bonds. A sealant that bonds well to one film may bond poorly to glass, metal or a coated surface. Surface preparation is covered in Substrate Cleaning Protocol for Thin-Film Devices: Solvents, UV-Ozone, Plasma and Queue Time and wetting in Why Your Ink Dewets: Surface Energy, Contact Angle and Wetting Before You Coat.

    3.  What Vacuum Does, and What It Does Not

    Air trapped between two layers can form voids or bubbles in the joint and can hold the layers apart. Pumping the stack down before pressing reduces the amount of gas available to be trapped. It does not guarantee a void-free joint: gas or vapor can also come from the materials themselves, from moisture or from reactions during heating, and the polymer must still flow and wet the surfaces.

    A published example from photovoltaic module lamination illustrates this. Wu and co-workers studied how lamination conditions affect EVA encapsulant stability, using curing level, void generation, chemical and optical stability and adhesion as indicators. They found that laminate stability increased with curing level up to an upper limit, beyond which voids formed, transmittance stability fell, discolouration appeared and interfaces became unstable; for the materials they tested, the best gel content range was 84–90% [4]. That result is specific to the EVA materials in the study, but it shows that more heat is not always better and that voids can form even in a vacuum laminator.

    Vacuum level, pump-down time before pressing, and the order in which vacuum and pressure are applied are therefore process variables to record and test, alongside temperature, pressure and dwell.

    4.  Sealing vs Laminating

    SealingLaminating
    Typical goalA joint along an edge or perimeter (for example, closing a pouch)Bonding over a whole area (for example, a cover sheet over a sample)
    Heat pathThrough a narrow seal areaThrough the full stack area
    Main risksWeak or channelled seal, edge deformationTrapped gas, voids, uneven thickness, thermal stress across the sample
    Role of vacuumRemoves air from inside a pouch before closingRemoves air between layers before pressing

    General comparison; actual practice depends on materials and geometry.

    Both use the same variables. Laminating usually heats the whole sample, so the thermal limits of every layer in the stack matter, not only those of the adhesive or sealant.

    5.  A Strong Joint Is Not a Barrier

    A strong joint is not the same as a barrier. Mechanical seal strength says nothing directly about how fast moisture or oxygen pass through the materials or along the interface.

    • Kempe and co-workers explain that thin-film photovoltaic technologies can be sensitive to corrosion from water vapor, and that modules typically use impermeable front and back sheets with an edge seal, often a desiccant-filled polyisobutylene, to slow ingress. They note that even the lowest-diffusivity transparent encapsulant materials are insufficient for the lifetime of a module on their own, and they used a calcium-film optical method to measure ingress [5].
    • Lewis and Weaver note that polymer substrates do not offer the same barrier performance as glass, so OLEDs on polymer substrates need thin-film barriers on both sides of the device layers for sufficient lifetimes [6].

    Barrier performance therefore depends on the materials and the design of the whole package, and must be measured with methods intended for permeation or ingress, not inferred from a successful seal.

    6.  Qualifying a Joint: Seal Strength, Damage and Repeatability

    ASTM F88/F88M covers the measurement of seal strength in flexible barrier materials. It measures the force required to separate a test strip containing a seal and identifies the failure mode; its scope includes seals between flexible materials and between flexible and rigid or semi-rigid materials [3]. Use it only where the specimen and seal fall within the standard’s scope. For other thin-film joints or full-area laminates, select a test method appropriate to the geometry and intended failure mode. ASTM F88/F88M describes seal strength as a quantitative measure for process validation, capability and control, and recommends consistent use of one test technique because unsupported, supported 90° and supported 180° configurations can give different results [3].

    For thin-film samples, qualification of a sealing or laminating step usually needs more than one check:

    CheckWhat it shows
    Seal strength and failure mode (for example, ASTM F88)Mechanical integrity of the joint; whether it fails in the seal or the material [3]
    Visual and optical inspection of the jointVoids, channels, wrinkles, deformation
    Device or film measurement before and afterWhether heat or pressure changed the sample
    Interface temperature, if it can be measuredActual thermal exposure rather than set-point [2]
    Repeat runs with recorded settingsRepeatability of the process
    Permeation or ingress tests where neededBarrier performance, which seal strength does not show [5]

    General qualification checklist.

    Thin-film sample considerations

    Application areas where these steps appear in the literature include photovoltaic modules [4][5] and flexible OLEDs [6]. These are general examples of the technique, not qualified uses of any particular instrument.

    7.  Levon™ HS150 and HS320-CTM-ZK: Published Specifications

    The Levon™ HS150 is a benchtop heat sealer with a 150 × 150 mm panel and a published temperature range of RT to 250°C. The Levon™ HS320-CTM-ZK is a vacuum heat sealer/laminator capable of sealing 300 × 300 mm samples, with a published temperature range of RT to 180°C, vacuum below 100 Pa, and adjustable vacuum and jacking pressure. These specifications describe the equipment, not a validated sealing recipe for every thin-film stack. Confirm material compatibility, seal geometry, operating conditions and the intended application with the supplier.

    SpecificationHS150HS320-CTM-ZK
    Type (page title)Benchtop heat sealer / laminatorVacuum heat sealer / laminator
    Sample / panel sizePanel size 150 × 150 mmCapable of sealing 300 × 300 mm samples
    Temperature rangeRT to 250 °CRT to 180 °C
    Resolution0.1 °C (after the temperature is stabilized)0.1 °C
    Accuracy / precisionAccuracy ≤±0.2 °CPrecision ±1 °C
    Published temperature-uniformity notation≤±2% (calculation basis not stated)≤±2% (calculation basis not stated)
    Temperature controlPID, dual-zoneNot stated
    Published vacuum level (test conditions not stated)Not statedBelow 100 Pa
    Adjustable parametersNot statedJacking pressure; vacuum level
    Compressed air / gas supply0.4–0.8 MPa; air inlet 6 mm OD0.4–0.8 MPa; gas interface 6 mm OD
    Other published featuresEmergency power cutoff; compact form factor for glove box integrationAutomatic heat sealing
    PowerAC 200–240 V, single-phase, 50 Hz, 2.0 kWAC 200–240 V, single-phase, 50 Hz, 2.0 kW
    Dimensions (W × D × H)200 × 200 × 340 mm; 10 kg560 × 650 × 400 mm; 70 kg

    Specifications as published on the Levon™ product pages on 24 October 2026. The supplied configuration is confirmed in the quotation. “Not stated” means the page does not give the value. The published ≤±2% uniformity notation is reproduced as stated; its reference basis and calculation method are not provided, so it should not be treated as a fully defined temperature tolerance.

    How this connects to the guide: the two models are not interchangeable. The HS320-CTM-ZK page publishes a vacuum level below 100 Pa and adjustable vacuum and jacking pressure, but does not state the validated operating pressure during sealing or the jacking-pressure range. The published temperature ranges and sample sizes also differ. As Section 2 explains, the interface temperature, dwell and pressure must be qualified for the intended process. The Levon™ HS150 Benchtop Heat Sealer and the Levon™ HS320-CTM-ZK Vacuum Heat Sealer can be discussed through the contact form.

    8.  Keep Exploring the Thin-Film Processing Knowledge Hub

    Links will be added as each article is published.

    Equipment

    Questions about a specific instrument can be sent through the contact form.

    9.  FAQ

    What controls the strength of a heat seal?

    For polyethylene films, mainly the maximum temperature reached at the interface [2].

    Does more pressure make a stronger seal?

    In the polyethylene study, slight pressure helped contact but higher pressure gave no benefit [2].

    Does a longer dwell time help?

    Only until the interface reaches the target temperature; beyond that it did not improve seal properties in that study [2].

    What does vacuum do in a vacuum heat sealer?

    It removes air before pressing, reducing trapped gas, but voids can still form from the materials or the process [4].

    How is seal strength measured?

    ASTM F88/F88M measures the force to separate a strip containing the seal and records the failure mode [3].

    Is a strong seal also a moisture barrier?

    No. Barrier performance depends on the materials and package design and must be measured separately [5][6].

    10.  References

    1Stehling FC, Meka P. Heat sealing of semicrystalline polymer films. II. Effect of melting distribution on heat-sealing behavior of polyolefins. J Appl Polym Sci. 1994;51(1):105–119. DOI: 10.1002/app.1994.070510112
    2Meka P, Stehling FC. Heat sealing of semicrystalline polymer films. I. Calculation and measurement of interfacial temperatures: effect of process variables on seal properties. J Appl Polym Sci. 1994;51(1):89–103. DOI: 10.1002/app.1994.070510111
    3ASTM International. ASTM F88/F88M-23: Standard Test Method for Seal Strength of Flexible Barrier Materials. West Conshohocken, PA: ASTM International; 2023. Available at: astm.org (accessed 24 October 2026)
    4Wu D, Wessel P, Zhu J, Montiel-Chicharro D, Betts TR, Mordvinkin A, et al. Influence of lamination conditions of EVA encapsulation on photovoltaic module durability. Materials. 2023;16(21):6945. DOI: 10.3390/ma16216945
    5Kempe MD, Dameron AA, Reese MO. Evaluation of moisture ingress from the perimeter of photovoltaic modules. Prog Photovolt Res Appl. 2014;22(11):1159–1171. DOI: 10.1002/pip.2374
    6Lewis JS, Weaver MS. Thin-film permeation-barrier technology for flexible organic light-emitting devices. IEEE J Sel Top Quantum Electron. 2004;10(1):45–57. DOI: 10.1109/JSTQE.2004.824072
    Disclaimer: ACS Material LLC believes that the information in this guide is accurate and represents the most current information available to us. ACS Material makes no representations or warranties, either express or implied, regarding the suitability of any Levon™ instrument for any particular purpose or the accuracy of the information listed here. Specifications are those published on the Levon™ product pages on 24 October 2026; “not stated” means the page does not give the value. Final configurations are confirmed at quotation. Findings from the cited studies apply to the materials and conditions in those studies. Heated platens and sealed samples can cause burns; follow your institution’s safety rules.